3QWY

CED-2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	KURCHATOV SNC BEAMLINE K4.4
Synchrotron site	KURCHATOV SNC
Beamline	K4.4
Spacegroup name	C 1 2 1
Unit cell lengths	105.211, 97.152, 71.096
Unit cell angles	90.00, 127.14, 90.00

Refinement procedure

Resolution	48.580 - 2.520
R-factor	0.20703
Rwork	0.204
R-free	0.26800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.034
RMSD bond angle	2.823
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASES
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	63.500
High resolution limit [Å]	2.500
Number of reflections	18916

Crystallization Conditions

crystal ID	method	pH	temperature	details
1