3QRL
Crystal Structure of the Taf14 YEATS domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.93 |
Spacegroup name | P 65 |
Unit cell lengths | 113.019, 113.019, 26.329 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.626 - 1.700 |
R-factor | 0.18988 |
Rwork | 0.188 |
R-free | 0.23508 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.516 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | autoSHARP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.626 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.032 | 0.408 |
Number of reflections | 21602 | |
<I/σ(I)> | 24.3 | 3.4 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 5.4 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 298 | 42.5% (v/v) PEG-600, 100 mM Sodium Citrate pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |