3QPX

Crystal structure of Fab C2507

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	125
Detector technology	CCD
Collection date	2008-01-07
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	60.150, 87.050, 100.310
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.525 - 2.000
R-factor	0.2266
Rwork	0.225
R-free	0.26390
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.970
Data reduction software	d*TREK
Data scaling software	d*TREK
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	66.000
High resolution limit [Å]	2.000
Rmerge	0.098
Number of reflections	35233
Completeness [%]	96.8
Redundancy	4.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	297	1.9 M (NH4)2SO4, 50 mM CdCl2, 0.1 M MES buffer, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 297K