3QNE
Candida albicans seryl-tRNA synthetase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-07 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 90.050, 90.050, 276.757 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 67.939 - 2.000 |
R-factor | 0.1673 |
Rwork | 0.165 |
R-free | 0.20650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dq0 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.157 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.100 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.069 | 0.230 |
Number of reflections | 43773 | |
<I/σ(I)> | 7.8 | 3.1 |
Completeness [%] | 95.7 | 78 |
Redundancy | 21.8 | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 298 | 3.2-3.4 M ammonium sulfate, 0-2% v/v glycerol, 100 mM MES/sodium, pH 5.6-5.8, VAPOR DIFFUSION, temperature 298K |