3QMQ
Crystal Structure of E. coli LsrG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-18 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.643, 83.397, 63.595 |
Unit cell angles | 90.00, 89.53, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.800 |
R-factor | 0.2063 |
Rwork | 0.204 |
R-free | 0.24290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | code 2GFF |
RMSD bond length | 0.023 |
RMSD bond angle | 1.969 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.1.3) |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 3.880 | 1.800 |
Rmerge | 0.127 | 0.086 | 0.420 |
Number of reflections | 42888 | ||
<I/σ(I)> | 5.3 | ||
Completeness [%] | 99.7 | 98.9 | 99.8 |
Redundancy | 3.6 | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | 6.5 | 298 | 1.65 M NaCitrate, pH 6.5, hanging drop, temperature 298K |