3Q9V
Crystal structure of rra c-terminal domain(123-221) from Deinococcus radiodurans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-12 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 49.251, 37.602, 48.573 |
Unit cell angles | 90.00, 113.92, 90.00 |
Refinement procedure
Resolution | 28.860 - 1.602 |
R-factor | 0.194947534671 |
Rwork | 0.193 |
R-free | 0.23029 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB Code 3Q9S |
RMSD bond length | 0.007 |
RMSD bond angle | 0.969 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.069 | 0.307 |
Number of reflections | 21545 | 2158 |
<I/σ(I)> | 26.5 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.8 | 293 | 0.1 M CH3COONa, 3.1 M NaCl, pH 4.8 |