3Q0X
N-terminal coiled-coil dimer domain of C. reinhardtii SAS-6 homolog Bld12p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-10 |
Detector | MAR225 |
Wavelength(s) | 1.00150 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.520, 79.800, 89.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.290 - 3.020 |
R-factor | 0.1972 |
Rwork | 0.196 |
R-free | 0.22850 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 56.290 | 3.100 | |
High resolution limit [Å] | 3.020 | 10.000 | 3.000 |
Rmerge | 0.173 | 0.077 | 0.742 |
Number of reflections | 10395 | 337 | 619 |
<I/σ(I)> | 10.79 | 20.2 | 2.6 |
Completeness [%] | 95.8 | 99.7 | 62.4 |
Redundancy | 11.23 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 298 | 100 mM TrisHCl, pH 8.5, 200 mM MgCl2, 20% PEG8000, 2% benzamidine, vapor diffusion, temperature 298K, VAPOR DIFFUSION |