3PSP
Crystal structure of PUL and PFU domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-07-10 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 61 |
Unit cell lengths | 102.495, 102.495, 73.306 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.624 - 2.422 |
R-factor | 0.1902 |
Rwork | 0.185 |
R-free | 0.23390 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.088 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 88.763 |
High resolution limit [Å] | 2.422 |
Number of reflections | 16781 |
Completeness [%] | 99.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293.15 | 0.15M Potassium bromide,30% w/v PEG 2000, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |