3PRK
INHIBITION OF PROTEINASE K BY METHOXYSUCCINYL-ALA-ALA-PRO-ALA-CHLOROMETHYL KETONE. AN X-RAY STUDY AT 2.2-ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 68.300, 68.300, 108.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 * - 2.200 |
R-factor | 0.198 |
RMSD bond length | 0.009 |
RMSD bond angle | 0.017 * |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Total number of observations | 53620 * |
Number of reflections | 11864 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | enzyme | 5 (%(w/v)) | |
2 | 1 | drop | Tris-HCl | 50 (mM) | |
3 | 1 | drop | 1 (mM) | ||
4 | 1 | reservoir | 0.75 (M) | ||
5 | 1 | reservoir | Tris-HCl | 50 (mM) |