3PO0
Crystal structure of SAMP1 from Haloferax volcanii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Wavelength(s) | 1.23985 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.881, 42.251, 43.568 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.193 - 1.550 |
R-factor | 0.2037 |
Rwork | 0.200 |
R-free | 0.24340 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.964 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.550 |
Number of reflections | 11712 |
Redundancy | 12.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | ||||
2 |