3PO0

Crystal structure of SAMP1 from Haloferax volcanii

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 6C1
Synchrotron site	PAL/PLS
Beamline	6C1
Temperature [K]	100
Wavelength(s)	1.23985
Spacegroup name	P 21 21 21
Unit cell lengths	41.881, 42.251, 43.568
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.193 - 1.550
R-factor	0.2037
Rwork	0.200
R-free	0.24340
Structure solution method	MAD
RMSD bond length	0.006
RMSD bond angle	0.964
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	PHENIX ((phenix.refine: 1.6.4_486))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.550
Number of reflections	11712
Redundancy	12.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
2