Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-2 |
| Synchrotron site | SSRL |
| Beamline | BL9-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-05-13 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97923 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.110, 62.620, 124.760 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 34.640 - 1.490 |
| R-factor | 0.17582 |
| Rwork | 0.174 |
| R-free | 0.20846 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.207 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.640 | 1.540 |
| High resolution limit [Å] | 1.490 | 1.490 |
| Rmerge | 0.076 | 0.032 |
| Number of reflections | 56717 | |
| <I/σ(I)> | 43.8 | |
| Completeness [%] | 98.9 | 94.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 7.5 | 298 | 20% PEG3350, 1M NaI, 0.1 M TrisHCl, pH 7.5, EVAPORATION, temperature 298K |
