3PJI
Crystal structure of AgamOBP22a at 1.7 angstrom in the open status for ligand binding.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-06 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.263, 37.702, 43.639 |
Unit cell angles | 90.00, 99.46, 90.00 |
Refinement procedure
Resolution | 25.424 - 1.704 |
R-factor | 0.1822 |
Rwork | 0.179 |
R-free | 0.20810 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.932 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.700 |
Number of reflections | 11797 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 1.8 M Ammonium citrate tribasic, 3.5% MPD, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |