3PIM
Crystal structure of Mxr1 from Saccharomyces cerevisiae in unusual oxidized form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-06-15 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 111.894, 111.894, 108.124 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 1.900 |
R-factor | 0.23754 |
Rwork | 0.236 |
R-free | 0.26448 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pil |
RMSD bond length | 0.011 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 59060 | |
Completeness [%] | 95.6 | 97.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 289 | 0.5M ammonium sulfate, 0.1M sodium citrate, 1.0M lithium sulfate, pH 5.6, VAPOR DIFFUSION, temperature 289K |