3PE7
Oligogalacturonate lyase in complex with manganese
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08ID-1 |
| Synchrotron site | CLSI |
| Beamline | 08ID-1 |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 66.650, 75.510, 78.510 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.650 |
| R-factor | 0.17827 |
| Rwork | 0.177 |
| R-free | 0.20682 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3c5m |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.249 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.690 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.085 | 0.350 |
| Number of reflections | 44824 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
