3PAU
CueO in the resting oxidized state
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-05-14 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 69.216, 73.113, 183.784 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.600 - 2.000 |
| R-factor | 0.21745 |
| Rwork | 0.215 |
| R-free | 0.26601 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1kv7 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.515 |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.600 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.175 | 0.502 |
| Number of reflections | 31821 | |
| <I/σ(I)> | 5.2 | 2.1 |
| Completeness [%] | 99.0 | 99.9 |
| Redundancy | 4.6 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 16% POLYETHYLENE GLYCOL 4000, 0.2 M AMMONIUM ACETATE, 0.1 M SODIUM ACETATE,, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
