3P83
Structure of the PCNA:RNase HII complex from Archaeoglobus fulgidus.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-09-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 149.670, 152.030, 90.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.540 - 3.050 |
R-factor | 0.1882 |
Rwork | 0.187 |
R-free | 0.21590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1RXM and PDB ENTRY 1I39 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.080 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | BUSTER (2.9.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.540 |
High resolution limit [Å] | 3.010 |
Rmerge | 0.116 |
Number of reflections | 39748 |
<I/σ(I)> | 15.8 |
Completeness [%] | 100.0 |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.2 | 293.15 | 18% PEG 3350, 196mM K2HPO4, pH 9.2, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |