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3P64

Time-dependent and Protein-directed In Situ Growth of Gold Nanoparticles in a Single Crystal of Lysozyme

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X12C
Synchrotron siteNSLS
BeamlineX12C
Temperature [K]123.2
Detector technologyCCD
Collection date2009-11-11
DetectorMAR CCD 165 mm
Wavelength(s)1.0988
Spacegroup nameP 43 21 2
Unit cell lengths78.567, 78.567, 36.947
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 1.300
R-factor0.2044
Rwork0.202
R-free0.23410
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle0.026
Data reduction softwareHKL-2000
Phasing softwareMOLREP (in the CCP4 Package)
Refinement softwareSHELXL-97
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.300
Rmerge0.079
Number of reflections28400
<I/σ(I)>48.8
Completeness [%]99.8
Redundancy27.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1EVAPORATION4.52986.5% NaCl (w/v) in 0.1 M sodium acetate, pH 4.5, EVAPORATION, temperature 298K

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