3P2W
Unliganded form of Polo-like kinase I Polo-box domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Collection date | 2009-08-06 |
Wavelength(s) | 0.9794 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 33.462, 98.882, 36.138 |
Unit cell angles | 90.00, 98.48, 90.00 |
Refinement procedure
Resolution | 49.450 - 1.660 |
R-factor | 0.20673 |
Rwork | 0.205 |
R-free | 0.23156 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1UMW (chain A) |
RMSD bond length | 0.006 |
RMSD bond angle | 0.973 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 49.450 |
High resolution limit [Å] | 1.660 |
Number of reflections | 26961 |
Completeness [%] | 96.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 100mM HEPES, 1.0-2.0M (NH4)2SO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |