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3OYD

Crystal structure of the Prototype Foamy Virus (PFV) intasome in complex with magnesium and the INSTI GS9160

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyAREA DETECTOR
Collection date2010-06-08
DetectorADSC
Wavelength(s)0.98011
Spacegroup nameP 41 21 2
Unit cell lengths159.530, 159.530, 123.580
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.880 - 2.540
R-factor0.2088
Rwork0.207
R-free0.23440
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3oyb
RMSD bond length0.012
RMSD bond angle1.602
Data reduction softwareMOSFLM
Data scaling softwareSCALA (3.3.16)
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]39.88239.8852.680
High resolution limit [Å]2.5408.0302.540
Rmerge0.0100.010
Total number of observations885442113
Number of reflections52902
<I/σ(I)>8.518.31.6
Completeness [%]99.897.299.9
Redundancy5.555.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52911.35 M ammonium sulfate, 25% (v/v) glycerol, 4.8% (v/v) 1,6-hexanediol, 50 mM Mes-NaOH, 1mM EDTA, pH 6.5, vapor diffusion, hanging drop, temperature 291K

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