3OWC
Crystal structure of GNAT superfamily protein PA2578 from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-18 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 41 |
Unit cell lengths | 71.095, 71.095, 97.952 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.900 |
R-factor | 0.17829 |
Rwork | 0.176 |
R-free | 0.21214 |
Structure solution method | SAD |
RMSD bond length | 0.020 |
RMSD bond angle | 2.047 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 (SOLVE/RESOLVE) |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.072 | 0.526 |
Number of reflections | 38282 | |
<I/σ(I)> | 27 | 2.3 |
Completeness [%] | 99.7 | 100 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 35% Tacsimate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |