3OWB
Crystal Structure of HSP90 with VER-49009
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-BM |
Synchrotron site | APS |
Beamline | 17-BM |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2005-10-27 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 65.339, 88.582, 99.546 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.050 |
R-factor | 0.1597 |
Rwork | 0.158 |
R-free | 0.19980 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | BUSTER-TNT (BUSTER-TNT 2.5.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.170 | 2.120 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 18609 | |
Completeness [%] | 98.9 | 91.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |