3OUJ
PHD2 with 2-Oxoglutarate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Collection date | 2006-11-29 |
Spacegroup name | P 41 |
Unit cell lengths | 72.298, 72.298, 46.496 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.330 - 2.300 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.25300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.145 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.113 | 0.330 |
Number of reflections | 10691 | |
<I/σ(I)> | 6.1 | 2.9 |
Completeness [%] | 99.1 | 95.1 |
Redundancy | 3.7 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.4 | 293 | 0.2 M AMMONIUM SULFATE, 28% PEG 8000, pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K |