3OTV
Crystal structure of the intracellular domain of Rv3910 from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-09-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.115872 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.037, 59.687, 145.063 |
Unit cell angles | 90.00, 97.21, 90.00 |
Refinement procedure
Resolution | 40.814 - 3.094 |
R-factor | 0.1924 |
Rwork | 0.189 |
R-free | 0.24840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ouk |
RMSD bond length | 0.010 |
RMSD bond angle | 1.303 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (- Phaser) |
Refinement software | ELVES |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.814 | 3.210 |
High resolution limit [Å] | 3.094 | 3.100 |
Rmerge | 0.631 | |
Number of reflections | 15986 | |
<I/σ(I)> | 9.9 | 1.73 |
Completeness [%] | 87.4 | 70.8 |
Redundancy | 3.4 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 0.7-0.8M succinate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |