3OSF
The structure of protozoan parasite Trichomonas vaginalis Myb2 in complex with MRE-2f-13 DNA
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-30 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.97622, 0.9788, 0.9790, 0.9686 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.941, 77.352, 84.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.654 - 2.032 |
R-factor | 0.209 |
Rwork | 0.206 |
R-free | 0.25790 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.397 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 2.030 | 5.510 | 2.030 |
Rmerge | 0.047 | ||
Number of reflections | 31586 | ||
Completeness [%] | 99.1 | 95.3 | 93.1 |
Redundancy | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 0.1M sodium cacodylate, 15% isopropanol, 25% PEG 4000, 10% glycerol, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |