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3ONU

Crystal Structure of P Domain from Norwalk Virus Strain Vietnam 026

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Temperature [K]77
Detector technologyCCD
Collection date2010-08-08
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths65.217, 79.111, 69.292
Unit cell angles90.00, 99.65, 90.00
Refinement procedure
Resolution22.695 - 1.395
R-factor0.1514
Rwork0.150
R-free0.16720
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.011
RMSD bond angle1.331
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.6.4_486))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.450
High resolution limit [Å]1.4001.400
Rmerge0.449
Number of reflections130975
<I/σ(I)>2
Completeness [%]95.269.6
Redundancy2.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52930.1 M Imidazole pH 6.5, 8.25% PEG 8000, 1% MPD , VAPOR DIFFUSION, HANGING DROP, temperature 293K

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