3ON9
The SECRET domain from Ectromelia virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Detector technology | CCD |
Collection date | 2009-11-04 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9793 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 72.416, 73.438, 112.412 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.740 - 1.570 |
R-factor | 0.1653 |
Rwork | 0.164 |
R-free | 0.19850 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.130 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXS |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.610 |
High resolution limit [Å] | 1.570 | 1.570 |
Number of reflections | 41455 | |
Completeness [%] | 98.3 | 87.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 0.4M Magnesium formate dehydrate, 0.1M Bis-Tris propane, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |