3OD7
Haemophilus influenzae ferric binding protein A -Iron Loaded
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 105 |
Detector technology | IMAGE PLATE |
Collection date | 2008-04-08 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 130.957, 52.515, 40.989 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.739 - 1.801 |
R-factor | 0.2049 |
Rwork | 0.203 |
R-free | 0.25030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1d9v |
RMSD bond length | 0.006 |
RMSD bond angle | 0.963 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.6.2_432)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.308 | |
Number of reflections | 26076 | |
Completeness [%] | 96.5 | 88.1 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 303 | 18% PEG 4000, 0.4M Imidazole/Malate, 0.2M NaCl, pH 6.6, VAPOR DIFFUSION, HANGING DROP, temperature 303K |