3OC3
Crystal structure of the Mot1 N-terminal domain in complex with TBP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-10 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.8726 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 99.260, 147.820, 103.440 |
Unit cell angles | 90.00, 94.52, 90.00 |
Refinement procedure
Resolution | 47.276 - 3.100 |
R-factor | 0.1899 |
Rwork | 0.187 |
R-free | 0.24210 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.866 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.200 |
High resolution limit [Å] | 3.100 | 3.100 |
Number of reflections | 54019 | |
Completeness [%] | 99.7 | 97.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 50mM Mes pH 6, 200mM Ammoniumacetate, 5% MPD, 4% PEG 3350, 200mM NDSB-201, VAPOR DIFFUSION, HANGING DROP, temperature 291K |