3O8V
Crystal Structure of the Tudor Domains from FXR1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-11 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97904 |
Spacegroup name | H 3 |
Unit cell lengths | 71.857, 71.857, 94.055 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.930 - 2.500 |
R-factor | 0.2201 |
Rwork | 0.218 |
R-free | 0.26120 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.760 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (refmac_5.6.0081) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 5.380 | 2.500 |
Rmerge | 0.074 | 0.067 | 0.549 |
Number of reflections | 6291 | ||
<I/σ(I)> | 19.1 | ||
Completeness [%] | 99.9 | 99.2 | 100 |
Redundancy | 3.9 | 4 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.8 | 291 | 1.4M Ammonium Sulfate, 0.1M HEPES pH 6.8, 0.25 M NaCl, 10 mM DTT, VAPOR DIFFUSION, SITTING DROP, temperature 291K |