3O7S
Crystal structure of Ru(p-cymene)/apo-Fr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-12 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 1.0 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.443, 181.443, 181.443 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.040 - 1.730 |
R-factor | 0.199 |
Rwork | 0.198 |
R-free | 0.21680 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.265 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.730 |
Number of reflections | 27184 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | AMMONIUM SULFATE, CADMIUM SLFATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |