3O03
Quaternary complex structure of gluconate 5-dehydrogenase from streptococcus suis type 2
Replaces: 3CXTExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 71.244, 75.272, 98.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.870 - 1.900 |
R-factor | 0.194 |
Rwork | 0.191 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cxr |
RMSD bond length | 0.018 |
RMSD bond angle | 1.637 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.870 | 25.870 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.068 | |
Number of reflections | 24607 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |