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3NX4

Crystal structure of the yhdH oxidoreductase from Salmonella enterica in complex with NADP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 21-ID-G
Synchrotron siteAPS
Beamline21-ID-G
Temperature [K]110
Detector technologyCCD
Collection date2010-04-25
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.97857
Spacegroup nameC 1 2 1
Unit cell lengths103.218, 122.364, 64.912
Unit cell angles90.00, 121.10, 90.00
Refinement procedure
Resolution37.042 - 1.900
R-factor0.1561
Rwork0.155
R-free0.19080
Structure solution methodSAD
RMSD bond length0.007
RMSD bond angle1.120
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSHELXS
Refinement softwarePHENIX (1.6.2_432)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.970
High resolution limit [Å]1.9004.0901.900
Rmerge0.1010.0710.546
Number of reflections51747
<I/σ(I)>11.523.112.56
Completeness [%]95.299.583.8
Redundancy9.410.56.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP729820% PEG3350, 200mM Ammonium Citrate, 10mM NADP, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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