3NVE
MMHFGN segment 138-143 from Syrian Hamster prion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-D |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-01-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 9.513, 11.784, 36.541 |
Unit cell angles | 90.00, 93.04, 90.00 |
Refinement procedure
Resolution | 36.490 - 1.700 |
R-factor | 0.206 |
Rwork | 0.196 |
R-free | 0.26880 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.024 |
RMSD bond angle | 1.904 |
Data scaling software | SCALEPACK |
Phasing software | PHASER (1.3.3) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 80.000 | 80.000 | 1.760 |
High resolution limit [Å] | 1.700 | 3.662 | 1.700 |
Rmerge | 0.162 | 0.163 | 0.150 |
Number of reflections | 939 | ||
<I/σ(I)> | 15.9 | ||
Completeness [%] | 97.2 | 99.1 | 88 |
Redundancy | 10.5 | 10.7 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 1.2 M Ammonium sulfate, 200 mM BisTris pH 7.5, vapor diffusion, hanging drop, temperature 298K |