Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2007-10-27 |
| Detector | PSI PILATUS 6M |
| Spacegroup name | P 1 |
| Unit cell lengths | 58.473, 73.206, 83.788 |
| Unit cell angles | 79.83, 69.45, 88.22 |
Refinement procedure
| Resolution | 48.549 - 1.836 |
| R-factor | 0.1908 |
| Rwork | 0.187 |
| R-free | 0.24600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3bmx |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.611 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.549 | 1.950 |
| High resolution limit [Å] | 1.836 | 1.840 |
| Rmerge | 0.081 | 0.417 |
| Number of reflections | 104555 | |
| <I/σ(I)> | 7.55 | 1.977 |
| Completeness [%] | 93.5 | 91.5 |
| Redundancy | 1.985 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 291 | 0.1M SODIUM ACETATE, 27% PEG 1000, pH 4.8, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
