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3NSZ

Human CK2 catalytic domain in complex with AMPPN

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2009-10-19
DetectorADSC QUANTUM 210
Wavelength(s)0.9999
Spacegroup nameP 21 21 21
Unit cell lengths49.382, 62.026, 117.061
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 1.300
R-factor0.1692
Rwork0.168
R-free0.18660
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle0.990
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareBUSTER (2.9.4)
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]1.300
Number of reflections89248
Completeness [%]99.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP629320-26% PEG 4000, 0.2 M AMMONIUM SULFATE, 0.1 M SODIUM CITRATE PH 6, 1 MM MGCL2 AND 10 MM AMPPNP, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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