3NQK
Crystal structure of a STRUCTURAL GENOMICS, UNKNOWN FUNCTION (BACOVA_03322) from Bacteroides ovatus at 2.61 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-07 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97937,0.97908 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 124.073, 124.073, 66.888 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.801 - 2.610 |
R-factor | 0.2 |
Rwork | 0.198 |
R-free | 0.23600 |
Structure solution method | MAD |
RMSD bond length | 0.015 |
RMSD bond angle | 0.917 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.15) |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.801 |
High resolution limit [Å] | 2.610 |
Number of reflections | 18340 |
Completeness [%] | 99.9 |
Redundancy | 11.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 277 | 0.200000000M (NH4)2Tartrate, 20.000000000% PEG-3350, No Buffer pH 6.6, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |