3NN9

REFINED ATOMIC STRUCTURES OF N9 SUBTYPE INFLUENZA VIRUS NEURAMINIDASE AND ESCAPE MUTANTS

Experimental procedure

Spacegroup name	I 4 3 2
Unit cell lengths	185.100, 185.100, 185.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.300
R-factor	0.178 *
Rwork	0.178
RMSD bond length	0.021
RMSD bond angle	4.000
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000 *
High resolution limit [Å]	2.200 *
Rmerge	0.121 *
Total number of observations	104979 *
Number of reflections	17915 *
Completeness [%]	68.6 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	6.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	potassium phosphate	1.7 (M)
2	1	drop	protein	10 (mg/ml)
3	1	reservoir	potassium phosphate	1.9 (M)