3NMW
Crystal structure of armadillo repeats domain of APC
Experimental procedure
Experimental method | SAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-25 |
Wavelength(s) | 0.97916 |
Spacegroup name | P 1 |
Unit cell lengths | 51.389, 52.682, 63.451 |
Unit cell angles | 90.31, 89.95, 95.16 |
Refinement procedure
Resolution | 50.000 - 1.600 |
R-factor | 0.16959 |
Rwork | 0.168 |
R-free | 0.20112 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.417 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.660 |
High resolution limit [Å] | 1.600 | 3.450 | 1.600 |
Rmerge | 0.075 | 0.060 | 0.342 |
Number of reflections | 165928 | ||
<I/σ(I)> | 13.3 | ||
Completeness [%] | 95.1 | 96.7 | 83.1 |
Redundancy | 1.9 | 2 | 1.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 287 | 25% PEG 3350, 180mM ammonium sulfate, pH 8.0, vapor diffusion, sitting drop, temperature 287K |