3NKJ
Crystal Structure of HP67 L61G
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2010-05-29 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.041, 39.544, 51.396 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.894 - 1.600 |
R-factor | 0.1854 |
Rwork | 0.182 |
R-free | 0.21860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yu5 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.101 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.894 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.042 | 0.126 |
Number of reflections | 7740 | |
Completeness [%] | 91.1 | 83 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 0.2 M SODIUM ACETATE, 0.1 M CACODYLATE, 30% POLYETHYLENE GLYCOL 10,000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |