3NCX
Crystal structure of EHEC O157:H7 intimin mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.771, 92.488, 100.048 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.977 - 2.600 |
R-factor | 0.2157 |
Rwork | 0.213 |
R-free | 0.26830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ncw |
RMSD bond length | 0.003 |
RMSD bond angle | 0.618 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.980 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.132 |
Number of reflections | 13058 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 15% PEG 20000, 0.1M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |