3NB0
Glucose-6-Phosphate activated form of Yeast Glycogen Synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-14 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.979 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 192.739, 206.982, 205.799 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.229 - 2.406 |
R-factor | 0.213 |
Rwork | 0.211 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3naz |
RMSD bond length | 0.004 |
RMSD bond angle | 0.737 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.087 | 0.552 |
Number of reflections | 157186 | |
<I/σ(I)> | 15.5 | |
Completeness [%] | 98.5 | 79.1 |
Redundancy | 4.8 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 293 | 0.1M Bis-Tris pH 6.2, 25% PEG 300, VAPOR DIFFUSION, HANGING DROP, temperature 293K |