3N89
KH domains
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-26 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 159.504, 102.241, 83.608 |
Unit cell angles | 90.00, 119.32, 90.00 |
Refinement procedure
Resolution | 48.113 - 2.789 |
Rwork | 0.259 |
R-free | 0.27600 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.214 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.100 | 3.070 |
High resolution limit [Å] | 2.790 | 2.790 |
Number of reflections | 28664 | |
<I/σ(I)> | 8.61 | 2.3 |
Redundancy | 2.7 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | Ammoniumsulfate, Hepes, Glycerol, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | Ammoniumsulfate, Hepes, Glycerol, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |