3N4V

apo APH(2")-IVa form III

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9795
Spacegroup name	P 1 21 1
Unit cell lengths	75.966, 65.119, 78.458
Unit cell angles	90.00, 91.68, 90.00

Refinement procedure

Resolution	42.183 - 2.400
R-factor	0.1965
Rwork	0.193
R-free	0.26310
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.153
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX ((phenix.refine: 1.5_2))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.183	2.500
High resolution limit [Å]	2.400	2.400
Rmerge	0.071	0.512
Number of reflections	28901
<I/σ(I)>	15.6	1.9
Completeness [%]	95.6	72

Crystallization Conditions

crystal ID	method	pH	temperature	details
1