3N49
Human FPPS COMPLEX WITH NOV_292
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-10-26 |
Detector | SATURN92 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 111.229, 111.229, 78.339 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.950 - 2.500 |
R-factor | 0.225 |
Rwork | 0.223 |
R-free | 0.27300 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNX |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.067 | 0.411 |
Number of reflections | 17572 | |
<I/σ(I)> | 13.3 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 14 | 14.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 292 | 1.2M sodium potassium phosphate, 25% glycerol, pH 5.3, VAPOR DIFFUSION, HANGING DROP, temperature 292K |