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3N32

The crystal structure of human Ubiquitin adduct with Zeise's salt

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyCCD
Collection date2008-10-10
DetectorADSC QUANTUM 315r
Wavelength(s)1.071
Spacegroup nameP 21 21 21
Unit cell lengths29.060, 40.450, 49.760
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.094 - 1.795
R-factor0.1841
Rwork0.181
R-free0.25750
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ubq
RMSD bond length0.008
RMSD bond angle1.093
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareILMILIONE (v.2.2)
Refinement softwarePHENIX ((phenix.refine: 1.6_289))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]31.3901.890
High resolution limit [Å]1.7951.795
Rmerge0.0400.198
Number of reflections5572
<I/σ(I)>27.47
Completeness [%]95.685.6
Redundancy4.44.41
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP729330% PEG 1450, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K

222036

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