3N1Q
Crystal Structure of DhhN bound to CDOFn3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU SATURN 944+ |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.715, 100.265, 97.260 |
Unit cell angles | 90.00, 98.98, 90.00 |
Refinement procedure
Resolution | 22.726 - 2.890 |
R-factor | 0.2396 |
Rwork | 0.237 |
R-free | 0.28760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.573 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 25.000 |
High resolution limit [Å] | 2.890 |
Number of reflections | 19402 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 298 | 20% peg3350, 200 mM Na(OAc), VAPOR DIFFUSION, temperature 298K |