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3N1N

Crystal structure of the complex of type I ribosome inactivating protein with guanine at 2.2A resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]292
Detector technologyIMAGE PLATE
Collection date2009-06-22
DetectorMAR scanner 345 mm plate
Wavelength(s)1.54
Spacegroup nameH 3
Unit cell lengths131.640, 131.640, 41.210
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution19.950 - 2.230
R-factor0.173
Rwork0.173
R-free0.19500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1aha
RMSD bond length0.009
RMSD bond angle1.900
Data reduction softwareAUTOMAR
Phasing softwareAMoRE
Refinement softwareCNS (0.9)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.250
High resolution limit [Å]2.2302.230
Number of reflections12622
Completeness [%]97.894.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5298Phosphate buffer, PEG6000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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