3N19
XenA - reduced
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Collection date | 2009-04-20 |
Wavelength(s) | 0.92 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 83.784, 158.031, 57.845 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.929 - 1.750 |
R-factor | 0.201 |
Rwork | 0.198 |
R-free | 0.25790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h8x |
RMSD bond length | 0.016 |
RMSD bond angle | 1.533 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.930 |
High resolution limit [Å] | 1.750 |
Number of reflections | 77884 |
Completeness [%] | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 290 | 1.5M Ammonium Sulfate, 100mM Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 290K |