3MYX
Crystal structure of a PSPTO_0244 (Protein with unknown function which belongs to Pfam DUF861 family) from Pseudomonas syringae pv. tomato str. DC3000 at 1.30 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-03 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97913,0.97879 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.584, 48.396, 80.454 |
Unit cell angles | 90.00, 108.21, 90.00 |
Refinement procedure
Resolution | 28.759 - 1.300 |
R-factor | 0.119 |
Rwork | 0.117 |
R-free | 0.14600 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.495 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0053) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.759 | 1.350 | |
High resolution limit [Å] | 1.300 | 2.800 | 1.300 |
Rmerge | 0.042 | 0.019 | 0.308 |
Number of reflections | 101752 | 19843 | 17364 |
<I/σ(I)> | 12.07 | 33.6 | 2.4 |
Completeness [%] | 96.4 | 97.4 | 80.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.3 | 277 | 0.2000M NH4Cl, 20.0000% PEG-3350, No Buffer pH 6.3, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |