3MYC
Crystal Structure of HP67 H41F - P212121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 2010-03-19 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.404, 37.107, 54.791 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.982 - 1.700 |
R-factor | 0.1847 |
Rwork | 0.181 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.872 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.982 | 1.831 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 6978 | |
Completeness [%] | 93.8 | 91 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2 M Ammonium Sulfate, 0.1 M 2-Morphinoethanesulfonic acid, 30% Polyethyleneglycol 8,000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |